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1060735-14-9

  • Product Name9-Phenyl-9h,9'h-[3,3']bicarbazolyl
  • Molecular FormulaC30H20N2
  • Molecular Weight408.5
  • Purity99%
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Product Details

Quick Details

  • CasNo： 1060735-14-9
  • Molecular Formula： C30H20N2
  • Purity： 99%

Good Quality Pharmaceutical Grade 9-Phenyl-9H,9'H-[3,3']bicarbazolyl 1060735-14-9

  • Molecular Formula:C30H20N2
  • Molecular Weight:408.502
  • Boiling Point:685.6±37.0 °C(Predicted) 
  • PKA:17.10±0.30(Predicted) 
  • PSA：20.72000 
  • Density:1.23±0.1 g/cm3(Predicted) 
  • LogP:8.08520 

9-Phenyl-9H,9'H-[3,3']bicarbazolyl(Cas 1060735-14-9) Usage

Application

9-phenyl-3,3’-bicarbazolyl is the intermediate to synthesis electronic materials, such as OLED.9-phenyl-3,3’-bicarbazolyl is a kind of organic electroluminescent materials to make OLED display screen, and this intermediate can be used in OLED series, such as Thiophene series, Fluorene series, Boronic Acid series and so on.

Isomeric SMILES: C1=CC=C(C=C1)N2C3=C(C=C(C=C3)C4=CC5=C(C=C4)NC6=CC=CC=C65)C7=CC=CC=C72  
InChIKey: GKTLHQFSIDFAJH-UHFFFAOYSA-N  
InChI: InChI=1S/C30H20N2/c1-2-8-22(9-3-1)32-29-13-7-5-11-24(29)26-19-21(15-17-30(26)32)20-14-16-28-25(18-20)23-10-4-6-12-27(23)31-28/h1-19,31H  

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1060735-14-9 Process route

3-bromo-9H-carbazole
1592-95-6

3-bromo-9H-carbazole

9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole
1126522-69-7

9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole

9-phenyl-3,3'-bicarbazole
1060735-14-9

9-phenyl-3,3'-bicarbazole

Conditions
Conditions Yield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); In water; toluene; for 5h; Inert atmosphere; Reflux;
87%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; for 4h; Inert atmosphere; Reflux;
80%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 24h; Inert atmosphere;
77%
With tetrakis(triphenylphosphine) palladium(0); sodium hydroxide; In tetrahydrofuran; water; at 80 ℃; for 12h; Inert atmosphere;
75%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; toluene; for 12h; Inert atmosphere; Reflux;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; toluene; for 12h; Reflux;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; for 12h; Inert atmosphere; Reflux;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; toluene; at 120 ℃; for 12h; Inert atmosphere;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; toluene; at 120 ℃; for 12h; Inert atmosphere;
68%
3-bromo-9H-carbazole; 9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole; With tetrakis(triphenylphosphine) palladium(0); In tetrahydrofuran; toluene; Inert atmosphere;
With potassium carbonate; In tetrahydrofuran; water; toluene; at 120 ℃; for 12h;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; toluene; for 12h; Reflux; Inert atmosphere;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; for 12h; Inert atmosphere; Reflux;
68%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; at 120 ℃; for 5h; Reflux;
62%
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0); In ethanol; toluene; at 74 - 80 ℃; for 5h; Inert atmosphere;
32.7%
3-iodocarbazole
16807-13-9

3-iodocarbazole

9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole
1126522-69-7

9-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)-9H-carbazole

9-phenyl-3,3'-bicarbazole
1060735-14-9

9-phenyl-3,3'-bicarbazole

Conditions
Conditions Yield
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0); In 1,4-dioxane; at 85 ℃; for 48h; Inert atmosphere;
74%
With potassium phosphate; tetrakis(triphenylphosphine) palladium(0); In 1,4-dioxane; at 85 ℃; for 48h; Inert atmosphere;
74%

1060735-14-9 Upstream products

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    N-phenyl-9H-carbazol-3-boronic acid

  • 1592-95-6
    1592-95-6

    3-bromo-9H-carbazole

  • 86-74-8
    86-74-8

    9H-carbazole

  • 108-86-1
    108-86-1

    bromobenzene

1060735-14-9 Downstream products

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    1060735-15-0

    9-phenyl-9'-[4-(10-phenyl-9-anthryl)phenyl]-3,3'-bi(9H-carbazole)

  • 1245801-46-0
    1245801-46-0

    9-phenyl-9'-[4-(5-phenyl-1,3,4-oxadiazole-2-yl)phenyl]-3,3'-bi(9H-carbazole)

  • 1245801-43-7
    1245801-43-7

    9-phenyl-9'-[4-(3-phenylquinoxalin-2-yl)phenyl]-3,3'-bi(9H-carbazol)

  • 1150-62-5
    1150-62-5

    N-phenylcarbazole

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