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500717-23-7

  • Product NameBis-(9,9-dimethyl-9h-fluoren-2-yl)-amine
  • Molecular FormulaC30H27N
  • Molecular Weight401.5
  • Purity99%
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Product Details

Quick Details

  • CasNo： 500717-23-7
  • Molecular Formula： C30H27N
  • Purity： 99%

Pharmaceutical Intermediates Bis-(9,9-dimethyl-9H-fluoren-2-yl)-amine 500717-23-7 Best Price

  • Molecular Formula:C30H27N
  • Molecular Weight:401.551
  • Melting Point:178℃ 
  • Boiling Point:571.0±39.0 °C(Predicted) 
  • PKA:1.01±0.40(Predicted) 
  • PSA：12.03000 
  • Density:1.146 
  • LogP:8.11580 

Bis-(9,9-diMethyl-9H-fluoren-2-yl)-aMine(Cas 500717-23-7) Usage

Uses

 Bis-(9,9-dimethyl-9H-fluoren-2-yl)-amine consists of two 9,9-dimethyl-9H-fluorene moieties connected by a secondary amine group. This compound has a rigid, planar structure and exhibits fluorescence properties. It finds applications in the development of organic light-emitting diodes (OLEDs) and other optoelectronic devices due to its favorable thermal and photophysical characteristics. Bis-(9,9-dimethyl-9H-fluoren-2-yl)-amine is considered an important material in the field of organic electronics and has been extensively studied for its potential in enhancing the performance of various electronic and photonic devices.

Isomeric SMILES: CC1(C2=CC=CC=C2C3=C1C=C(C=C3)NC4=CC5=C(C=C4)C6=CC=CC=C6C5(C)C)C  
InChIKey: LCSMGMWMTSWXDD-UHFFFAOYSA-N  
InChI: InChI=1S/C30H27N/c1-29(2)25-11-7-5-9-21(25)23-15-13-19(17-27(23)29)31-20-14-16-24-22-10-6-8-12-26(22)30(3,4)28(24)18-20/h5-18,31H,1-4H3  

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500717-23-7 Process route

9,9-dimethyl-9H-fluoren-2-ylamine
108714-73-4

9,9-dimethyl-9H-fluoren-2-ylamine

2-bromo-9,9-dimethyl-9H-fluorene
28320-31-2

2-bromo-9,9-dimethyl-9H-fluorene

N-(9,9-dimethyl-9H-fluoren- 2-yl)-9,9-dimethyl-9H-fluoren-2-amine
500717-23-7

N-(9,9-dimethyl-9H-fluoren- 2-yl)-9,9-dimethyl-9H-fluoren-2-amine

Conditions
Conditions Yield
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; XPhos; In toluene; at 105 - 110 ℃; for 2.5h; Inert atmosphere;
84%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate; In toluene; at 85 ℃; for 3h;
81%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate; In toluene; for 5h; Inert atmosphere; Reflux;
63.1%
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; In toluene; at 90 ℃; for 3h; Inert atmosphere;
61%
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 90 ℃; for 19h; Inert atmosphere;
60%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; In toluene; at 110 ℃; for 24h; Inert atmosphere;
 
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate; In toluene; at 100 ℃; for 8h;
 
tert-butyl bis(9,9-dimethyl-9H-fluoren-7-yl)carbamate
1185882-60-3

tert-butyl bis(9,9-dimethyl-9H-fluoren-7-yl)carbamate

N-(9,9-dimethyl-9H-fluoren- 2-yl)-9,9-dimethyl-9H-fluoren-2-amine
500717-23-7

N-(9,9-dimethyl-9H-fluoren- 2-yl)-9,9-dimethyl-9H-fluoren-2-amine

Conditions
Conditions Yield
With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;
95%
tert-butyl bis(9,9-dimethyl-9H-fluoren-7-yl)carbamate; With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 0.166667h;
With sodium hydroxide; In tetrahydrofuran; dichloromethane; water;
95%
With sodium hydroxide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
 
With trifluoroacetic acid; In tetrahydrofuran;
 

500717-23-7 Upstream products

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    tert-butyl bis(9,9-dimethyl-9H-fluoren-7-yl)carbamate

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    2-iodo-9,9-dimethyl-9H-fluorene

  • 108714-73-4
    108714-73-4

    9,9-dimethyl-9H-fluoren-2-ylamine

  • 28320-31-2
    28320-31-2

    2-bromo-9,9-dimethyl-9H-fluorene

500717-23-7 Downstream products

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    4-(2-(bis(9,9-dimethyl-9H-fluoren-7-yl)amino)-9,9-spirobifluoren-7-yl)benzaldehyde

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