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Product Details
Description |
Dibenzofuran-4-boronic acid (DBFBA) is a boronic acid that has been used as a cross-coupling agent in the Suzuki coupling reaction. It has been shown to have low efficiency, but advances in this area have been made through the use of methanol extraction and photophysical properties. DBFBA is often coupled with imidazole derivatives to form anti-inflammatory compounds. The bond cleavage and hydrogen bonding properties of DBFBA make it a good target for drug synthesis. |
Chemical Properties |
off-white to beige powder |
Isomeric SMILES | B(C1=C2C(=CC=C1)C3=CC=CC=C3O2)(O)O |
Exact Mass | 212.0644743 g/mol |
Monoisotopic Mass | 212.0644743 g/mol |
Complexity | 259 |
InChI:InChI=1/C6H5BF2O2/c8-4-1-2-5(7(10)11)6(9)3-4/h1-3,10-11H
Two blue fluorescent phenanthroimidazole...
Organozinc pivalates, a recently develop...
Increasing the boronic acid to 3.0 molar equiv … acid, use of 1.5 molar equiv of dibenzofuran-4-boronic acid resulted in a slow reaction (46 h). In this case increasing the boronic …
The invention provides a compound, an el...
PURPOSE: A condensed cyclic compound is ...
The invention discloses a synthesis meth...
4-dibenzofurylboronic acid
Conditions | Yield |
---|---|
With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 3h; Inert atmosphere;
In tetrahydrofuran; at -78 - 20 ℃;
|
79% |
With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 3h; Inert atmosphere;
In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
|
79% |
With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃; for 24h; Inert atmosphere;
In tetrahydrofuran; at -78 - 20 ℃; for 2h; Inert atmosphere;
With hydrogenchloride;
|
78.6% |
Butyl-Li, 1) Dibenzofuran, Ae., 2) Trimethylborat, 3) wss. H2SO4;
|
dibenzofuran
Triisopropyl borate
4-dibenzofurylboronic acid
Conditions | Yield |
---|---|
dibenzofuran; With n-butyllithium; In tetrahydrofuran; hexane; at -68 - -20 ℃; for 1h; Inert atmosphere;
Triisopropyl borate; In tetrahydrofuran; hexane; at -68 - 20 ℃; for 5h;
With hydrogenchloride; In tetrahydrofuran; hexane; water; ethyl acetate;
|
dibenzofuran
Triisopropyl borate
4-bromodibenzofuran
Trimethyl borate
3-dibenzofuran-4-yl-2-methoxy-benzaldehyde
N-(dibenzofuran-4-yl)-N-phenyl-amine
dibenzo[b,d]furan-4-yl(phenyl)methanone
3-{1-[3-(tert-butyldiphenylsilanyloxy)-propyl]-1H-pyrrolo[2,3-b]pyridin-3-yl}-4-dibenzofuran-4-yl-pyrrole-2,5-dione
CAS:1001911-63-2
Molecular Formula:C<sub>18</sub> H<sub>14</sub> BNO<sub>2</sub>
Molecular Weight:287.1
CAS:89827-45-2