932710-63-9

  • Product NameBis(di-tert-butyl)-4-dimethylaminophenylphosphine
  • Molecular FormulaC16H28NP
  • Molecular Weight265.37
  • Purity99%
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Product Details

Quick Details

  • CasNo: 932710-63-9
  • Molecular Formula: C16H28NP
  • Purity: 99%

Export Bis(di-tert-butyl)-4-dimethylaminophenylphosphine 932710-63-9 In Bulk Supply

  • Molecular Formula:C16H28NP
  • Molecular Weight:265.379
  • Melting Point:57-61°C 
  • Boiling Point:349.1±25.0 °C(Predicted) 
  • PKA:4.73±0.24(Predicted) 
  • PSA:16.83000 
  • LogP:4.45680 

Bis(di-tert-butyl)-4-dimethylaminophenylphosphine(Cas 932710-63-9) Usage

Use

Bis(di-tert-butyl)-4-dimethylaminophenylphosphine is an organophosphine compound and can be used as an organophosphine ligand.

Reaction

Ligand used in a highly-active palladium precatalyst for the efficient amination of aryl chloride. Ligand used in the palladium-catalyzed annulations under microwave enhanced conditions.

Uses

Amphos can be used as an electrophotographic photoreceptor, process cartridge, and image forming electrode.

InChI:InChI=1S/C16H28NP/c1-15(2,3)18(16(4,5)6)14-11-9-13(10-12-14)17(7)8/h9-12H,1-8H3

932710-63-9 Relevant articles

Preparation method for bis[di-tert-butyl(4-dimethylaminophenyl)phosphine]dichloropalladium

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Paragraph 0057; 0059; 0060, (2018/11/03)

The invention discloses a preparation me...

Method for synthesizing [4-(N,N-dimethylamino)phenyl]dialkylphosphine

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Paragraph 0009; 0010, (2017/10/31)

The invention discloses a method for syn...

Di-tert-butyl - 4 - dimethyl amino phosphonate and double (di-tert-butyl - 4 - dimethyl amino phosphonate) preparation method of catalysts

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Paragraph 0061-0063, (2017/08/25)

The invention provides a preparing metho...

NOVEL CATALYSTS

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Page/Page column 71, (2012/06/01)

The present invention provides novel com...

932710-63-9 Process route

di-tert-butylphosphonium chloride

di-tert-butylphosphonium chloride

<i>N</i>,<i>N</i>-dimethyl-aniline
121-69-7,77733-26-7

N,N-dimethyl-aniline

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine
932710-63-9

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine

Conditions
Conditions Yield
With dmap; copper (I) acetate; In toluene; at 120 ℃; for 8h; Temperature; Inert atmosphere;
96%
di(tert-butyl)chlorophosphine
13716-10-4

di(tert-butyl)chlorophosphine

4-N,N-dimethylaminophenyl magnesium chloride
108949-55-9

4-N,N-dimethylaminophenyl magnesium chloride

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine
932710-63-9

(4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine

Conditions
Conditions Yield
di(tert-butyl)chlorophosphine; 4-N,N-dimethylaminophenyl magnesium chloride; at -30 ℃; for 0.166667h; Inert atmosphere;
With ammonium chloride; In water; at -30 ℃; for 0.5h;
85%

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