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Product Details
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Chemical Properties |
Off-white powder |
InChI:InChI=1/C24H15Br/c25-24-21-13-5-3-11-19(21)23(20-12-4-6-14-22(20)24)18-15-7-9-16-8-1-2-10-17(16)18/h1-15H
The present specification relates to an ...
A double-deck silsesquioxane derivative ...
The invention relates to a blue light el...
The invention belongs to the technical f...
10-(naphthalen-1-yl)anthracene
10-bromo-9-(naphthalene-1'-yl)anthracene
| Conditions | Yield |
|---|---|
|
With N-Bromosuccinimide; In chloroform; at 60 ℃; for 3h; Inert atmosphere;
|
98% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 2h;
|
97.5% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 2h;
|
97.5% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
|
92.2% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
|
92% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
|
92% |
|
With N-Bromosuccinimide; In dichloromethane; for 16h; Inert atmosphere;
|
91% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 24h; Inert atmosphere; Reflux;
|
90% |
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With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 24h; Reflux;
|
90% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide;
|
89% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 0.5h;
|
89% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; for 0.5h;
|
89% |
|
With bromine; In dichloromethane;
|
88.3% |
|
With N-Bromosuccinimide; In chloroform; for 3h; Reflux;
|
87% |
|
With N-Bromosuccinimide; In 1,2-dichloro-ethane; at 0 - 10 ℃; for 2h; Inert atmosphere;
|
84.97% |
|
With N-Bromosuccinimide; In N,N-dimethyl-formamide; chlorobenzene; at 85 ℃; for 3h;
|
82% |
|
With bromine; In dichloromethane; at 0 ℃;
|
76% |
|
With bromine; In dichloromethane; at 0 - 20 ℃;
|
76% |
|
With bromine; In dichloromethane; at 0 - 20 ℃;
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76% |
|
With bromine; In dichloromethane; at 0 ℃;
|
75% |
9,10-Dibromoanthracene
1-Naphthylboronic acid
10-bromo-9-(naphthalene-1'-yl)anthracene
| Conditions | Yield |
|---|---|
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 2h;
|
80% |
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In water; toluene; at 60 ℃; for 0.333333h; Inert atmosphere;
|
76.89% |
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; at 50 - 90 ℃; Inert atmosphere;
|
62.1% |
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With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In toluene; for 24h; Inert atmosphere; Reflux;
|
62% |
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With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In water; toluene; for 24h; Inert atmosphere; Reflux;
|
62% |
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With tetrakis(triphenylphosphine) palladium(0); sodium carbonate; In ethanol; toluene; at 100 ℃; for 12h; Inert atmosphere;
|
42% |
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With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; at 80 ℃; for 8h; Inert atmosphere;
|
|
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With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water;
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9,10-Dibromoanthracene
1-Naphthylboronic acid
9-Bromoanthracene
10-(naphthalen-1-yl)anthracene
4,4,5,5-tetramethyl-2-(10-naphthalene-1-yl-anthracene-9-yl)-[1,3,2]dioxaborolane
9-(naphthalen-1-yl)anthracen-10-yl-10-boronic acid
C37H23N
C55H45NSi
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CAS:28320-31-2
Molecular Formula:C<sub>15</sub>H<sub>13</sub>Br
Molecular Weight:273.17
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CAS:604-53-5
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CAS:864377-31-1
