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Next, the preformed 3-phenylnaphthalen-1-ol 6 was subjected to reaction with 2-phenylindole … This indicates that 3-phenylnaphthalen-1-ol is not an intermediate for the generation of 3, …
This research successfully achieved a Cu(II)-catalyzed 6π-photocyclization of non-6πsubstrates. The photoenolization converts ortho-alkylphenyl alkynl ketones into a triene-type intermediate which undergoes the subsequent 6π-photocyclization to give napht
… into the formation of 4, the preformed 3-phenylnaphthalen-1-ol 6 was treated with indole 4 d … It did not give the desired product 4 l (Scheme 5a), indicating that 3-phenylnaphthalen-1-ol …
2-Methylpropionic anhydride
phenylacetylene
phenylacetyl chloride
3-phenylnaphthalen-1-ol
isobutyric Acid
| Conditions | Yield |
|---|---|
|
2-Methylpropionic anhydride; phenylacetylene; phenylacetyl chloride; at 190 ℃; for 48h; Inert atmosphere;
With potassium hydroxide; In water; at 100 ℃; for 13 - 15h;
|
70% |
3-bromo-1-hydroxynaphthalene
phenylboronic acid
3-phenylnaphthalen-1-ol
| Conditions | Yield |
|---|---|
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
|
75% |
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
|
75% |
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
|
75% |
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
|
75% |
|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; at 65 ℃; for 18h;
|
73% |
3,4-diphenyl-crotonic acid
bromobenzene
(E)-N,N-diethyl-3-phenylbut-2-enamide
3,4-dihydro-3-cyano-3-phenyl-1H-2-benzopyran-1-one
2-phenyl[1,4]naphthoquinone
3-phenylnaphthalene-1,2-dione
2-phenylnaphthalene
<3-Phenyl-naphthyl-(1)-oxy>-essigsaeure
CAS:120-74-1
Molecular Formula:C<sub>8</sub>H<sub>10</sub>O<sub>2</sub>
Molecular Weight:138.16
CAS:13029-09-9
Molecular Formula:C<sub>12</sub>H<sub>8</sub>Br<sub>2</sub>
Molecular Weight:312
