30069-65-9

  • Product Name3-Phenylnaphthalen-1-ol
  • Molecular FormulaC16H12O
  • Molecular Weight220.26
  • Purity99%
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Product Details

Quick Details

  • CasNo: 30069-65-9
  • Molecular Formula: C16H12O
  • Purity: 99%

High Purity 3-phenylnaphthalen-1-ol 30069-65-9 with Competitive Price

  • Molecular Formula:C16H12O
  • Molecular Weight:220.271
  • Melting Point:96-97.5 °C(Solv: chloroform (67-66-3); hexane (110-54-3)) 
  • Boiling Point:417.4±24.0 °C(Predicted) 
  • PKA:9.28±0.40(Predicted) 
  • PSA:20.23000 
  • Density:1.176±0.06 g/cm3(Predicted) 
  • LogP:4.21240 

30069-65-9 Relevant articles

Dual Palladium/Scandium Catalysis toward Rotationally Hindered C3‐Naphthylated Indoles from β‐Alkynyl Ketones and o‐Alkynyl Anilines

Dan Wang, Shi-Chao Wang, Wen-Juan Hao, Shu-Jiang Tu, Bo Jiang

Chinese Journal of Chemistry, Volume39, Issue1 January 2021 Pages 106-114

Next, the preformed 3-phenylnaphthalen-1-ol 6 was subjected to reaction with 2-phenylindole … This indicates that 3-phenylnaphthalen-1-ol is not an intermediate for the generation of 3, …

Cu(II)-Catalyzed 6π-Photocyclization of Non-6πSubstrates

Zhang, Yanbin,Jin, Ruiwen,Kang, Wenjie,Guo, Hao

, p. 5502 - 5505 (2020/07/08)

This research successfully achieved a Cu(II)-catalyzed 6π-photocyclization of non-6πsubstrates. The photoenolization converts ortho-alkylphenyl alkynl ketones into a triene-type intermediate which undergoes the subsequent 6π-photocyclization to give napht

Selective Syntheses of Benzo[b]carbazoles and C3-Substituted Indoles via Tunable Catalytic Annulations of β-Alkynyl Ketones with Indoles

Dan Wang, Shi-Chao Wang, Wen-Juan Hao, Shu-Jiang Tu, Bo Jiang

Advanced Synthesis & Catalysis, Volume362, Issue16 August 19, 2020 Pages 3416-3422

… into the formation of 4, the preformed 3-phenylnaphthalen-1-ol 6 was treated with indole 4 d … It did not give the desired product 4 l (Scheme 5a), indicating that 3-phenylnaphthalen-1-ol …

30069-65-9 Process route

2-Methylpropionic anhydride
97-72-3

2-Methylpropionic anhydride

phenylacetylene
536-74-3

phenylacetylene

phenylacetyl chloride
103-80-0

phenylacetyl chloride

3-phenylnaphthalen-1-ol
30069-65-9

3-phenylnaphthalen-1-ol

isobutyric Acid
79-31-2

isobutyric Acid

Conditions
Conditions Yield
2-Methylpropionic anhydride; phenylacetylene; phenylacetyl chloride; at 190 ℃; for 48h; Inert atmosphere;
With potassium hydroxide; In water; at 100 ℃; for 13 - 15h;
70%
3-bromo-1-hydroxynaphthalene
90767-17-2

3-bromo-1-hydroxynaphthalene

phenylboronic acid
98-80-6

phenylboronic acid

3-phenylnaphthalen-1-ol
30069-65-9

3-phenylnaphthalen-1-ol

Conditions
Conditions Yield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
75%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
75%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
75%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; toluene; for 16h; Reflux;
75%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; at 65 ℃; for 18h;
73%

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